Oxanilate

Ox`an´i`late


n.1.(Chem.) A salt of oxanilic acid.
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C(alpha), N-Dilithiophenylhydrazones were prepared in excess lithium diisopropylamide, {LDA), and condensed with ethyl oxanilates or ethyl oxamate to give C-acylated intermediates that could be isolated or cyclized directly with aqueous hydrochloric acid/ tetrahydrofuran (THF) to the targeted 1H-pyrazole-5-carbox-amides.
The preparation of dilithiated C(alpha), N-carbomethoxyhydrazones in excess LDA is quite straightforward along with their condensation with ethyl oxanilates to afford Cacylated intermediates that can be isolated.
9:45 The Preparation of 5-Isoxazolecarboxamides and Related Compounds from the Condensation and Cyclization of Dilithiated Oximes or Polylithiated Hydrazones with Polylithiated Oxanilates, J.
Several dilithiated C([alpha]), O-oximes were prepared in excess lithium diisopropylamide and condensed with lithiated ethyl oxanilates to give C-acylated intermediates that could be isolated and separately cyclized with aqueous acid to afford substituted 5-isoxazole-carboxamides.
Several dilithiated C([alpha]), O-oximes or C([alpha]), N-hydrazones were prepared in excess lithium diisopropylamide and condensed with either dilithiated ethyl oximate or lithiated ethyl oxanilates to give C-acylated intermediates that could be isolated or occasionally cyclized directly with aqueous acid to afford substituted 5-isoxazole-carboxamides or pyrazole-5-carboxamides.