The sodium
methoxide are used widely in several applications.
Summary: The sodium
methoxide are used widely in several applications.
The reaction mixture was then cooled to about 15 , and the pH was adjusted to 9-10 by the addition of 3 M sodium
methoxide in methanol, with simultaneous cooling.
Fatty acids were derived based on Hernandez-Galan (2011), using chloroform and sodium
methoxide. Fatty acid methyl esters (FAME) were analyzed using a gas chromatograph (Agilent mod.
The calcium
methoxide ring opening polymerization (ROP) of CL was reported in the literature [5].
The extracted lipids were dried using a rotary evaporator (N-110, Tokyo Rikakikai Co., Ltd, Tokyo, Japan) in vacuum and converted to methyl esters by base-catalyzed trans-esterification with sodium
methoxide for 2 h at 30[degrees]C [17].
(2015) and as follow: 4mL of a sodium
methoxide (2%) solution were added to the fat, vortexed every 5min during 15min at room temperature, then 4mL of H2SO4: methanol solution (1:2), vortexed a few seconds and vortexed again before adding 2mL of distilled water.
In addition, besides the mechanical mixing, ultra-sonication was used to reduce the processing time and the amount of
methoxide needed to perform a base catalyzed transesterification.
Sodium
methoxide, methanol and acetone were purchased from Merck.
[1.sup]H NMR spectrum (Figure 3) showed signal at 3.65 ppm correlated to
methoxide protons of the ester function and confirming the obtaining of the methyl ester of babassu while the triplet at 2.28 ppm is correlated to the a-methylene protons to ester.
Suwanthai, Optimization of Refined Bleached and deodorized Palm Oil Biodiesel Production Using Calcium
Methoxide Catalyst by Response Surface Methodology, Department of Chemistry, Kasetsart University, Bangkok, Thailand, 2014.